作者
Fan Zhang, Jan Ilavsky, Gabrielle G Long, John PG Quintana, Andrew J Allen, Pete R Jemian
发表日期
2010/5
期刊
Metallurgical and Materials Transactions A
卷号
41
页码范围
1151-1158
出版商
Springer US
简介
Absolute calibration of small-angle scattering (SAS) intensity data (measured in terms of the differential scattering cross section per unit sample volume per unit solid angle) is essential for many important aspects of quantitative SAS analysis, such as obtaining the number density, volume fraction, and specific surface area of the scatterers. It also enables scattering data from different instruments (light, X-ray, or neutron scattering) to be combined, and it can even be useful to detect the existence of artifacts in the experimental data. Different primary or secondary calibration methods are available. In the latter case, absolute intensity calibration requires a stable artifact with the necessary scattering profile. Glassy carbon has sometimes been selected as this intensity calibration standard. Here we review the spatial homogeneity and temporal stability of one type of commercially available glassy carbon that is …
引用总数
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F Zhang, J Ilavsky, GG Long, JPG Quintana, AJ Allen… - Metallurgical and Materials Transactions A, 2010