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The processes of (n)ZVI/AC((nano)zero valent iron/activated carbon)micro-electrolysis were applied for nitrate removal from groundwater, aiming to reduce nitrate to N₂, an environmentally friendly end product. (n)ZVI was utilized and combined with selected commercial AC to form the micro-electrolysis. Effect of different operational parameters, including reductant dosage, (n)ZVI/AC ratios, and reaction pH, on nitrate and TN removal were cleared. The results showed that nZVI presents higher reaction activities than ZVI in micro-electrolysis. With the increase of the (n)ZVI/AC mass ration from 1:2 to 2:1, the TN removal increased from 16.8% to 38.9%, then declined with the further increase of the ratio. The nitrate removal was negatively correlated with the initial pH of the solution. Compared to ZVI particles, even with a lower dosage, nZVI presented 100% nitrate removal at acidic and neutral pH conditions, and TN …