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This study investigates the effects of the initial grain size and temperature (ranging from room temperature to 1100 °C) on the mechanical properties and microstructure evolution of Ti₂AlC MAX phase. A Hall-Petch like relationship is observed between compressive strength and the grain size below brittle-to-plastic transition temperature (BPTT). However, the compressive strength of fine-grained MAX phase decreases more rapidly with increasing temperature resulting in inverse Hall-Petch effect above BPTT. Results from postmortem EBSD analysis reveal complex microstructural evolution in both fine- and coarse-grained microstructures during loading at different temperatures. The pronounced drop in compressive strength for fine-grained microstructures at temperatures close to BPTT is attributed to creep induced grain boundary sliding resulting in texture development with more grains oriented for easy slip. In …