作者
Mohd Farhan Khan, Akhter H Ansari, M Hameedullah, Ejaz Ahmad, Fohad Mabood Husain, Qamar Zia, Umair Baig, Mohd Rehan Zaheer, Mohammad Mezbaul Alam, Abu Mustafa Khan, Zeid A AlOthman, Iqbal Ahmad, Ghulam Md Ashraf, Gjumrakch Aliev
发表日期
2016/6/28
期刊
Scientific reports
卷号
6
期号
1
页码范围
1-12
出版商
Nature Publishing Group
简介
The effect of mechanical stirring on sol-gel synthesis of thorn-like ZnO nanoparticles (ZnO-NPs) and antimicrobial activities is successfully reported in this study. The in-house synthesized nanoparticles were characterized by XRD, SEM, TEM, FTIR, TGA, DSC and UV-visible spectroscopy. The X-Ray Diffraction analysis revealed the wurtzite crystal lattice for ZnO-NPs with no impurities present. The diametric measurements of the synthesized thorn-like ZnO-NPs (morphology assessed by SEM) were well accounted to be less than 50 nm with the help of TEM. Relative decrease in aspect ratio was observed on increasing the agitation speed. The UV-visible spectroscopy showed the absorption peaks of the ZnO-NPs existed in both UVA and UVB region. A hypsochromic shift in λmax was observed when stirring pace was increased from 500 rpm to 2000 rpm. The FTIR spectroscopy showed the absorption bands of the …
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