作者
RA Oliver, MJ Kappers, J Sumner, R Datta, CJ Humphreys
发表日期
2006/4/1
期刊
Journal of Crystal Growth
卷号
289
期号
2
页码范围
506-514
出版商
North-Holland
简介
Fast-turnaround, accurate methods for the assessment of threading dislocation (TD) densities in GaN are an essential research tool. Here, we present an in situ surface treatment in which GaN is exposed to a SiH4 flux at 860°C in the presence of NH3. Following a 240s exposure to SiH4, pits associated with screw or mixed-type TD were found to have more than doubled in diameter, as measured by atomic force microscopy (AFM). These pits are associated with step-edge terminations. Additional small pits had appeared, not associated with step-edge terminations, which are believed to relate to edge-type TDs. The total density of pits on the treated surface corresponded to the total dislocation density measured by transmission electron microscopy. Pits related to edge-type TDs are often overlooked in AFM of untreated GaN. As the SiH4 treatment time is increased, the measured dislocation density initially increases …
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