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The aim of this study was to test the hypothesis that magnesium supplementation influences the physical performance of volleyball players, as the efficacy of this approach remains questionable. Twenty-five professional male volleyball players were assigned randomly to experimental (350 mg Mg · d^–1, 4 weeks) and control groups (500 mg maltodextrin · d^–1, 4 weeks) maintaining inter-group homogeneity of urinary magnesium. Erythrocyte, plasma and urinary magnesium levels, plasma creatine kinase activity, lactate production, maximal oxygen uptake (VO₂ max) and plyometric (squat jump, countermovement jump, countermovement jump with arm swing) and isokinetic (peak torque, potency and total work) performances were evaluated before (T₀) and after (T₁) supplementation. Levels of erythrocyte and urinary magnesium and creatine kinase activity and VO₂ max remained within normal ranges in both groups …