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Graphene nanoplates (GNPs) can be used as a platform for homogeneous distribution of adsorbent nanoparticles to improve electron exchange and ion transport for heavy-metal adsorption. In this study, we report a facile thermal decomposition route to fabricate a graphene-supported Fe–Mg oxide composite. The prepared composite was characterized using scanning electron microscopy, transmission electron microscopy, energy-dispersive spectrometry, X-ray diffraction, and X-ray photoelectron spectroscopy. Batch experiments were carried out to evaluate the arsenic adsorption behavior of the GNP/Fe–Mg oxide composite. Both the Langmuir and Freundlich models were employed to describe the adsorption isotherm, in which the sorption kinetics of the arsenic adsorption process by the composite was found to be pseudo-second-order. Furthermore, the reusability and regeneration of the adsorbent were …