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Because antibiotic-containing wastewaters are able to contaminate all environmental matrices (e.g. water bodies, soil, etc.), a special attention should be paid on developing appropriate materials for their remediation. Herein, the novel nanocomposite (NC) of Fe₃O₄-g-CN@PEI-β-CD was synthesized and employed effectively for the adsorptive removal of tetracycline (TC), the second most produced and employed antibiotic around the world. The successful fabrication of the nanocomposite with a high specific surface area (57.12 m²/g) was confirmed using XRD, SEM, TEM, FTIR, TGA, EDX, and BET analyses. The Fe₃O₄-g-CN@PEI-β-CD NC exhibited fast adsorption rates towards TC and maximum adsorption capacity on the basis of the Langmuir model reached 833.33 mg g⁻¹, much higher than that reported by different carbon- and/or nano-based materials. The adsorption process was modeled using the …