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In the present work, nickel-titanium (NiTi) shape memory alloys (SMAs) is joined to 304 stainless steel (SS) using friction stir welding (FSW) using process parameters of 400 rpm and a constant tool translation speed of 75 mm/min. The macrostructure of the dissimilar weld showed some surface tunneling defects but there were regions of the weld that were defect free and without evidence of intermetallics at the interface. The weld stir zone (SZ) showed grain refinement compared to both base materials (BM). NiTi side of the joint showed very fine thermomechanical affected zone (TMAZ) and absence of a distinct heat affected (HAZ) zone, resulting in very little variation in microhardness. SS side of the weld showed typical FSW microstructural zones with higher microhardness in the SZ (270 HV) compared to BM (185 HV). Tensile testing of the weld showed a small initial plateau region, characteristic of shape memory …