作者
Kai Yang, SH Xu, XC Zeng, JH Lu, SH Guo, XL Li
发表日期
2004/1/1
期刊
Chinese Journal of Structural Chemistry
卷号
23
期号
6
页码范围
631-634
出版商
CHINESE JOURNAL STRUCTURAL CHEMISTRY
简介
The title compound (C29H50O2, M-r = 430.69) was isolated from the algae Halimeda xishaensis collected from the South China Sea. Its crystal structure was determined by single-crystal X-ray diffraction for the first time. The crystal belongs to orthorhombic, space group P2(1)2(1)2(1) with a = 8.1560(13), b = 10.7861(18), c = 29.973(5) Angstrom, V = 2636.8(8) Angstrom(3), Z = 4, D-c = 1.085 g/cm(3), F(000) = 960, mu(Mo-Kalpha) = 4.533 mm(-1), lambda = 0.71073 Angstrom, S = 1.061, (Deltarho)(max) 0.382 and (Deltarho)(min) = -0.244 e/Angstrom(3). The structure was refined to R = 0.0561 and wR = 0.1553 for 2711 observed reflections with I > 2sigma(I). X-ray diffraction analysis reveals that the title compound has two beta-OH groups, and the side chain is saturated. There exist two intermolecular hydrogen bonds between three molecules.
引用总数
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学术搜索中的文章
K Yang, SH Xu, XC Zeng, JH Lu, SH Guo, XL Li - Chinese Journal of Structural Chemistry, 2004
杨凯, 徐石海, 曾向潮, 吕俊华, 郭书好, 李筱玲 - 结构化学, 2004