作者
Inas Issa, Christoph Gammer, Stefan Kolitsch, Anton Hohenwarter, Peter J Imrich, Reinhard Pippan, Daniel Kiener
发表日期
2021/9/1
期刊
Materials today
卷号
48
页码范围
29-37
出版商
Elsevier
简介
We report a length-scale-controlled Brittle-Ductile Transition giving rise to significant toughening of a commonly brittle material. Using quantitative in-situ Transmission Electron Microscopy (TEM) fracture experiments at room temperature on single crystal Silicon, we find that large samples fracture concordant with the brittle bulk behavior at a stress intensity K I C~ 1 M P a. m 1/2. Below characteristic dimensions of about 250 nm, however, the fracture toughness strikingly increases inversely with size to at least triple. As evidenced from advanced in-situ TEM nanoscale strain mapping the stresses at the crack tip approach the theoretical strength. At the same time, below this critical transition length nucleation and propagation of dislocations was observed, shielding the crack tip and enabling the unprecedented rise in fracture toughness. These first time in-situ TEM observations in nanoscale Silicon at room temperature …
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I Issa, C Gammer, S Kolitsch, A Hohenwarter, PJ Imrich… - Materials today, 2021