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The dissimilar welds joint of 2.25Cr-1Mo steel and lean duplex LDX2101 steel was prepared using the Gas Tungsten Arc Welding (GTAW) process and employing the Inconel 617 filler. The microstructural stability of the dissimilar welds joint (DWJ) was studied using the optical microscope and field emission scanning electron microscope (FESEM) for as-welded (AW) and post-weld heat treatment (PWHT) condition. The PWHT was employed at 760 °C (PW 1) and 810 °C (PW 2) for 2 h of duration. The application of the heat-treatment resulted in the formation of the soft zone at the interface of weld metal and HAZ in 2.25 Cr-1Mo side, i.e., low Cr side. The mechanical behavior of the DWJs was also studied for AW and PWHT condition. A measurable change in the width and hardness of the soft and hard zones was measured with an increase in PWHT temperature. For weld metal, the minimum average hardness …