Bringing the on‐line control and optimization of semibatch emulsion copolymerization to the pilot plant

A Zubov, O Naeem, SO Hauger… - Macromolecular …, 2017 - Wiley Online Library
Copolymerization The subject of our study is a pilot plant with a 2.3 m 3 semibatch reactor
jacketed for cooling purposes, as depicted in Figure 2. In order to implement model based soft-…

Inline Raman Spectroscopy of an Emulsion Copolymerization in an Industrial Pilot Plant Using Indirect Hard Modeling

JMM Faust, W Gerlinger, O Naeem… - Chemie Ingenieur …, 2022 - Wiley Online Library
pilot plant operation, only HPLC measurements of styrene are available. The experiments
were run in a 2300-L pilot plant … Only styrene is measured for the pilot plant experiments and a …

Process Model for Styrene and n-Butyl Acrylate Emulsion Copolymerization in Smart-Scale Tubular Reactor

R Pokorný, A Zubov, P Matuška, F Lueth… - Industrial & …, 2016 - ACS Publications
… During the development of the mathematical model of Sty/BA emulsion copolymerization,
we made several simplifying assumptions that are generally accepted and validated by the …

Model-based control of continuous emulsion co-polymerization in a lab-scale tubular reactor

P Joy, K Rossow, F Jung, HU Moritz, W Pauer… - Journal of Process …, 2019 - Elsevier
… In this section, a brief description of the experimental setup as well as an overview of emulsion
polymerization is given. A detailed description of emulsion polymerization can be found in …

Modular, flexible, and continuous plant for radical polymerization in aqueous solution

D Kohlmann, MC Chevrel, S Hoppe… - Macromolecular …, 2016 - Wiley Online Library
… experiments of a pilot plant meeting the requirements of F 3 Factory plant for the specific …
dealing with radical copolymerization were scarce and focused on emulsion process.61 We …

Optimal nonlinear control of an industrial emulsion polymerization reactor

ID Gil, JC Vargas, JP Corriou - Chemical Engineering Research and …, 2016 - Elsevier
emulsion copolymerization, using iterative dynamic programming with an objective function
that included a term for the copolymer … In this section, a simulation of a pilot plant reactor from …

Bilevel Model Predictive Control of a Semi-Batch Emulsion Copolymerisation Reactor

E Kjetså - 2017 - ntnuopen.ntnu.no
… on a pilot plant. The RECOBA project’s objective is to use an on-line model predictive control
of complex batch processes for the production of emulsion polymers, among other things. …

On-line monitoring and control of emulsion polymerization reactors

S Hamzehlou, JM Asua - Advances in Chemical Engineering, 2020 - Elsevier
Emulsion polymers have gained industrial interest because on one hand, they substitute …
the emulsion polymers is controlled by multiple characteristics including copolymer composition…

Renewable feedstocks in emulsion polymerization: Coating and adhesive applications

M Aguirre, S Hamzehlou, E González… - Advances in Chemical …, 2020 - Elsevier
… They proposed to use conjugated linoleic acid (CLA), which comes from plant oils, by
emulsion copolymerization with St and BA. Due to the high price of CLA, they used the cheap …

Dynamic optimization of an emulsion copolymerization process for product quality using a deterministic kinetic model with embedded Monte Carlo simulations

JMM Faust, T Chaloupka, J Kosek, A Mhamdi… - Computers & Chemical …, 2019 - Elsevier
… We present the dynamic optimization of an emulsion copolymerization process described
by a deterministic kinetic ordinary differential equation model including a stochastic Monte …