[HTML][HTML] Accurate measurement of thin film mechanical properties using nanoindentation

S Zak, COW Trost, P Kreiml, MJ Cordill - Journal of Materials Research, 2022 - Springer
Journal of Materials Research, 2022Springer
For decades, nanoindentation has been used for measuring mechanical properties of films
with the widely used assumption that if the indentation depth does not exceed 10% of the
film thickness, the substrate influence is negligible. The 10% rule was originally deduced for
much thicker metallic films on steel substrates and involved only the hardness
measurement. Thus, the boundaries of usability for measuring thin film elastic modulus may
differ. Two known material systems of Mo and MoTa thin films on Si substrates are examined …
Abstract
For decades, nanoindentation has been used for measuring mechanical properties of films with the widely used assumption that if the indentation depth does not exceed 10% of the film thickness, the substrate influence is negligible. The 10% rule was originally deduced for much thicker metallic films on steel substrates and involved only the hardness measurement. Thus, the boundaries of usability for measuring thin film elastic modulus may differ. Two known material systems of Mo and MoTa thin films on Si substrates are examined with nanoindentation and numerical modeling to show the limitations in measuring elastic moduli. An assessment of the hardness and elastic modulus as a function of contact depth and accurate modeling of the film/substrate deformation confirms the 10% rule for hardness measurements. For elastic modulus, the indentation depths should be much smaller. Results provide a recommended testing protocol for accurate assessment of thin film elastic modulus using nanoindentation.
Graphical abstract
Springer
以上显示的是最相近的搜索结果。 查看全部搜索结果