In this paper, we investigate the reflection properties of different interior surfaces in the 92–110 GHz sub-Terahertz (THz) band. The measurements were conducted in an indoor environment by placing the surface in a specular configuration between the Transmitter (Tx) and Receiver (Rx) and collecting a large set of data by offsetting the Tx and Rx in parallel to the surface. The measurements were performed using an Agilent N5230A Vector-Network-Analyzer (VNA). In particular, we present a statistical analysis in the frequency domain to show how frequency selective each surface reflection is and how constant this behaviour is across the whole data set. We introduce the Power-Delay-Profile (PDP) to characterize the multipath behaviour of the channel and calculate the Root-Mean-Square (RMS) delay spread. The measurement results provide a good insight for future propagation work to be done for the development of indoor communications systems at sub-THz frequencies.