Deep eutectic solvent-based air-assisted liquid–liquid microextraction of lead in gasoline samples followed by graphite furnace atomic absorption spectrometry

SM Sorouraddin, MA Farajzadeh, H Dastoori… - Journal of the Iranian …, 2022 - Springer
This paper describes determination of lead in gasoline by graphite furnace atomic
absorption spectrometry after application of an air-assisted liquid–liquid microextraction
method using deep eutectic solvent. In this study, for the first time, a ternary deep eutectic
solvent was synthesized from menthol, mandelic acid, and glycolic acid and was used as a
complexing agent and an extraction solvent, simultaneously. Under optimized conditions,
the proposed method made possible the determination of lead in the range of 5–50 ng L− 1 …

Derivatization and deep eutectic solvent-based air–assisted liquid–liquid microextraction of salbutamol in exhaled breath condensate samples followed by gas …

A Jouyban, MA Farajzadeh, M Khoubnasabjafari… - … of Pharmaceutical and …, 2020 - Elsevier
A microwave-induced air–assisted liquid–liquid microextraction method has been proposed
for the pretreatment/quantization of salbutamol in exhaled breath condensate (EBC)
samples prior to gas chromatography-mass spectrometry. In this procedure, 1-fluoro-2, 4-
dinitrobenzene and N, N-diethylethanolammonium chloride: dichloroacetic acid: octanoic
acid deep eutectic solvent were exploited as derivatization reagent and extraction solvent,
respectively. A mixture of the sample solution and pyridine was transferred into a test tube …
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