Synthesis, physicochemical and antimicrobial properties of rhenium (I) tricarbonyl complexes of isatin Schiff bases
AA Ikotun, AA Owoseni… - African Journal of …, 2021 - academicjournals.org
The Schiff base of isatin and sulphanilamide (L1; C 14 H 11 N 3 O 3 S) was prepared and
reacted with Re (CO) 5 X (X= Cl and Br) in toluene to give [Re (C 14 H 10 N 2 O)(CO) 3
X](X= Cl, 1 and X= Br, 2). The prepared Schiff base of isatin and 4-methoxyaniline (L2; C 15
H 12 N 2 O 2) was reacted with Re (CO) 5 X in toluene to give [Re (C 14 H 10 N 2 O)(CO) 3
X], where X= Cl, 3 and X= Br, 4. L2 and Re (CO) 5 Br were refluxed in dry toluene under
nitrogen and recrystallized to give [Re (C 15 H 12 N 2 O 2)(CO) 3 Br]. 1/2 C 2 H 5 OH (5) …
reacted with Re (CO) 5 X (X= Cl and Br) in toluene to give [Re (C 14 H 10 N 2 O)(CO) 3
X](X= Cl, 1 and X= Br, 2). The prepared Schiff base of isatin and 4-methoxyaniline (L2; C 15
H 12 N 2 O 2) was reacted with Re (CO) 5 X in toluene to give [Re (C 14 H 10 N 2 O)(CO) 3
X], where X= Cl, 3 and X= Br, 4. L2 and Re (CO) 5 Br were refluxed in dry toluene under
nitrogen and recrystallized to give [Re (C 15 H 12 N 2 O 2)(CO) 3 Br]. 1/2 C 2 H 5 OH (5) …
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