Forces between alumina surfaces in salt solutions: non‐DLVO forces and the implications for colloidal processing

WA Ducker, Z Xu, DR Clarke… - Journal of the American …, 1994 - Wiley Online Library
Journal of the American Ceramic Society, 1994Wiley Online Library
Direct measurements of the forces between basal (0001) surfaces of sapphire in salt
solutions are presented. The measurements reveal the presence of forces in addition to
those described by classical DLVO theory. At pH 7.2 in 0.01 M NaBr solution, we find an
additional short‐range oscillatory force with periodicity approximately equal to twice the
diameter of a water molecule. At pH 3 we find an additional strong, short‐range, monotonic,
repulsive force and a long‐range attractive force over a range of NaBr concentrations from …
Direct measurements of the forces between basal (0001) surfaces of sapphire in salt solutions are presented. The measurements reveal the presence of forces in addition to those described by classical DLVO theory. At pH 7.2 in 0.01M NaBr solution, we find an additional short‐range oscillatory force with periodicity approximately equal to twice the diameter of a water molecule. At pH 3 we find an additional strong, short‐range, monotonic, repulsive force and a long‐range attractive force over a range of NaBr concentrations from 0.001 M to 0.1 M. Both monotonic forces are approximately exponential, with decay lengths of 0.55 and 12 nm, respectively. The short‐range force is analogous to hydration forces previously measured on negatively charged surfaces. This force would provide plasticity to alumina slurries and is suggested to be the force responsible for the anomalous viscosity and consolidation behavior of alumina slurries at high salt concentrations.
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