K3PO4-mediated one-pot synthesis of symmetrical trithiocarbonates
B Movassagh, S Alapour - Journal of Sulfur Chemistry, 2013 - Taylor & Francis
B Movassagh, S Alapour
Journal of Sulfur Chemistry, 2013•Taylor & Francis… A new procedure has been developed for synthesis of symmetrical trithiocarbonates by
one-pot reaction of carbon disulfide, and various alkyl halides in dimethylformamide using K 3
PO 4 as an inexpensive and effective reagent. … We have now developed an easy and highly
convenient methodology for one-pot synthesis of a variety of symmetrical dialkyl trithiocarbonates
by the reaction of alkyl halides with CS 2 in an aerobic atmosphere mediated by anhydrous K 3
PO 4 in dry dimethylformamide (DMF) at 50C. … In conclusion, the K 3 PO 4 -mediated …
one-pot reaction of carbon disulfide, and various alkyl halides in dimethylformamide using K 3
PO 4 as an inexpensive and effective reagent. … We have now developed an easy and highly
convenient methodology for one-pot synthesis of a variety of symmetrical dialkyl trithiocarbonates
by the reaction of alkyl halides with CS 2 in an aerobic atmosphere mediated by anhydrous K 3
PO 4 in dry dimethylformamide (DMF) at 50C. … In conclusion, the K 3 PO 4 -mediated …
A new procedure has been developed for synthesis of symmetrical trithiocarbonates by one-pot reaction of carbon disulfide, and various alkyl halides in dimethylformamide using K3PO4 as an inexpensive and effective reagent.
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