This paper describes an electrochemical method for the preparation of ⁵⁷Co source to be used in quality evaluation of nuclear fuel rods. The electrolytic cell, the experimental set up used and the process of deposition are described. The effect of various parameters such as pH of the electrolyte, bath temperature, current density, content of cobalt in the bath, electrolyte volume in the cell and deposition time were investigated and optimized for maximum deposition. The texture and morphology of the electrodeposited samples were examined by X-ray diffraction (XRD), SEM and EDS analyses. Sources containing ∼370 MBq (10 mCi) ⁵⁷Co on a circular copper foil of 4 mm diameter could be prepared and encapsulated in an aluminum capsule. Quality assurance tests performed to ensure non-leachability, uniform distribution of activity and stability of the sources gave satisfactory results.