Quantification of probe–sample interactions of a scanning thermal microscope using a nanofabricated calibration sample having programmable size

Y Ge, Y Zhang, JA Booth, JMR Weaver… - …, 2016 - iopscience.iop.org
Y Ge, Y Zhang, JA Booth, JMR Weaver, PS Dobson
Nanotechnology, 2016iopscience.iop.org
We report a method for quantifying scanning thermal microscopy (SThM) probe–sample
thermal interactions in air using a novel temperature calibration device. This new device has
been designed, fabricated and characterised using SThM to provide an accurate and
spatially variable temperature distribution that can be used as a temperature reference due
to its unique design. The device was characterised by means of a microfabricated SThM
probe operating in passive mode. This data was interpreted using a heat transfer model …
Abstract
We report a method for quantifying scanning thermal microscopy (SThM) probe–sample thermal interactions in air using a novel temperature calibration device. This new device has been designed, fabricated and characterised using SThM to provide an accurate and spatially variable temperature distribution that can be used as a temperature reference due to its unique design. The device was characterised by means of a microfabricated SThM probe operating in passive mode. This data was interpreted using a heat transfer model, built to describe the thermal interactions during a SThM thermal scan. This permitted the thermal contact resistance between the SThM tip and the device to be determined as 8.33× 10 5 KW− 1. It also permitted the probe–sample contact radius to be clarified as being the same size as the probe's tip radius of curvature. Finally, the data were used in the construction of a lumped-system steady state model for the SThM probe and its potential applications were addressed.
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