[ie, Ho 2 (Ti 1.33 Ho 0.67) O 6.67], comparing samples synthesized through two different
routes. Neutron powder diffraction and electron diffraction reveal that the previously reported
defect fluorite phase has short-range pyrochlore ordering, in that there are domains in which
the Ho and Ho∕ Ti sublattices are distinct. By contrast, a sample prepared through a floating
zone method has long-range ordering of these sublattices. Despite the differences in crystal …