Synthesis of alkoxybenzylmethylsilanes and polybenzylmethylsiloxane polymers on their basis
SA Milenin, AA Kalinina, VV Gorodov… - Russian Chemical …, 2015 - Springer
SA Milenin, AA Kalinina, VV Gorodov, NG Vasilenko, MI Buzin, AM Muzafarov
Russian Chemical Bulletin, 2015•SpringerAn efficient solvent-free procedure for the preparation of alkoxybenzylmethylsilanes by
organomagnesium synthesis was developed. The reaction conditions gave the high yields
of the target products. A number of benzylmethylsiloxane polymers was synthesized by
polycondensation of alkoxybenzylmethylsilanes in anhydrous acetic acid. The products
obtained can become a good alternative to phenylsiloxanes in some practical applications.
organomagnesium synthesis was developed. The reaction conditions gave the high yields
of the target products. A number of benzylmethylsiloxane polymers was synthesized by
polycondensation of alkoxybenzylmethylsilanes in anhydrous acetic acid. The products
obtained can become a good alternative to phenylsiloxanes in some practical applications.
Abstract
An efficient solvent-free procedure for the preparation of alkoxybenzylmethylsilanes by organomagnesium synthesis was developed. The reaction conditions gave the high yields of the target products. A number of benzylmethylsiloxane polymers was synthesized by polycondensation of alkoxybenzylmethylsilanes in anhydrous acetic acid. The products obtained can become a good alternative to phenylsiloxanes in some practical applications.
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