ZnO/ZnAl2O4 Nanocomposite Films Studied by X‐Ray Diffraction, FTIR, and X‐Ray Photoelectron Spectroscopy
S Iaiche, A Djelloul - Journal of Spectroscopy, 2015 - Wiley Online Library
Journal of Spectroscopy, 2015•Wiley Online Library
ZnO/ZnAl2O4 nanocomposite films were synthesised by ultrasonic spray pyrolysis (USP) by
extracting Al2O (SO4) 2 oxide with zinc chloride hydrate in deionised water. The sample was
then subjected to heat treatment at 650° C and 700° C for 1 h, which led to the formation of
the spinel oxide (ZnAl2O4) and wurtzite (ZnO) phases. Al2 (SO4) 3· 18H2O salt was
transformed into aluminum oxide sulfate Al2O (SO4) 2, which is an intermediary
decomposition product, by calcination at 795° C for 3 h. The structures of the synthesised …
extracting Al2O (SO4) 2 oxide with zinc chloride hydrate in deionised water. The sample was
then subjected to heat treatment at 650° C and 700° C for 1 h, which led to the formation of
the spinel oxide (ZnAl2O4) and wurtzite (ZnO) phases. Al2 (SO4) 3· 18H2O salt was
transformed into aluminum oxide sulfate Al2O (SO4) 2, which is an intermediary
decomposition product, by calcination at 795° C for 3 h. The structures of the synthesised …
ZnO/ZnAl2O4 nanocomposite films were synthesised by ultrasonic spray pyrolysis (USP) by extracting Al2O(SO4)2 oxide with zinc chloride hydrate in deionised water. The sample was then subjected to heat treatment at 650°C and 700°C for 1 h, which led to the formation of the spinel oxide (ZnAl2O4) and wurtzite (ZnO) phases. Al2(SO4)3·18H2O salt was transformed into aluminum oxide sulfate Al2O(SO4)2, which is an intermediary decomposition product, by calcination at 795°C for 3 h. The structures of the synthesised ZnO/ZnAl2O4 films were confirmed by XRD, FTIR, and X‐ray photoelectron spectroscopy (XPS). XPS spectra of the major Zn, Al, and O photoelectron lines and the major X‐ray induced Zn LMM Auger lines for ZnO/ZnAl2O4 are presented.
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