Synthesis and structural evaluation of freeze-cast porous alumina

DF Souza, EHM Nunes, DS Pimenta… - Materials …, 2014 - Elsevier
In this work we fabricated alumina samples by the freeze-casting technique using tert-
butanol as the solvent. The prepared materials were examined by scanning electron …

Macroporous alumina structures tailored by freeze-casting using naphthalene–camphor as freezing vehicle

LD Lacerda, DF Souza, EHM Nunes, M Houmard - Ceramics International, 2018 - Elsevier
Freeze-casting is a promising technique for fabricating macroporous ceramics because it is
an environmentally friendly, cost effective, and easy scale-up method. Several freezing …

Microstructural characterization and gas permeation performance of freeze-cast alumina supports

DF Souza, EHM Nunes, JA Queiroga… - Journal of the European …, 2018 - Elsevier
One of the major challenges for obtaining asymmetric membranes has been the preparation
of ceramic supports with tailored pore structures. The methods commonly used for …

Effect of titania addition on the properties of freeze-cast alumina samples

AMA Silva, EHM Nunes, DF Souza, DL Martens… - Ceramics …, 2015 - Elsevier
This work investigated the behavior of TiO 2-containing α-Al 2 O 3 samples prepared by the
freeze-casting technique. Camphene and liquid nitrogen were used as the solvent and …

[HTML][HTML] Freeze-casting applied to ceramic materials: a short review of the influence of processing parameters

L Santos, JRS Silva, JM Cartaxo, AM Rodrigues… - Cerâmica, 2021 - SciELO Brasil
In recent years there is a high interest in the freeze-casting process because it is a simple,
economical, and environmentally friendly method for obtaining highly porous materials. Most …

Effects of alcohol additives on pore structure and morphology of freeze-cast ceramics

Z Jing, Y Zhang, K Zhou, D Zhang - … of Nonferrous Metals Society of China, 2014 - Elsevier
The porous alumina ceramics with lamellar structure were fabricated successfully by freeze
casting. The viscosities of alumina slurries, pore structures, porosities and mechanical …

A review of fabrication strategies and applications of porous ceramics prepared by freeze-casting method

R Liu, T Xu, C Wang - Ceramics International, 2016 - Elsevier
Freeze casting is a promising technique to fabricate porous materials with complex pore
shapes and component geometries. Of particular interest are the unique structure and …

Influence of cryogenic drying conditions on hierarchical porous structure of aluminum oxide systems

K Sinkó, B Kobzi, J Sinclaire, A Baris… - … and Mesoporous Materials, 2015 - Elsevier
Highly porous alumina systems were aimed to produce by low energy-consuming sol–gel
and freeze drying techniques. A 3D molecular gel structure derived by sol–gel method is …

Freeze casting of aqueous alumina slurries with glycerol for porous ceramics

Y Zhang, L Hu, J Han, Z Jiang - Ceramics international, 2010 - Elsevier
Experiments have been performed to show that the mechanical properties of alumina
porous ceramics may be improved by introducing glycerol into the raw slurries and then …

Pore structure of porous ceramics synthesized from water-based slurry by freeze-dry process

T Fukasawa, ZY Deng, M Ando, T Ohji… - Journal of Materials …, 2001 - Springer
A unique porous ceramic with complex pore structure was synthesized by the freeze-dry
process. A water-based ceramic slurry was frozen while controlling the growth direction of …