Determination of polychlorinated biphenyls by chemical ionization mass spectrometry

T Cairns, EG Siegmund - Analytical Chemistry, 1981 - ACS Publications
GCMS techniques using chemical ionization have been em-ployed to characterize by
molecular weight composition, five FDA reference Aroclor standards. The results Indicated …

Development of methane positive chemical ionization gas chromatography mass spectrometry procedures to determine polychlorinated biphenyl

RD Voyksner, JT Bursey, TW Pack… - Analytical …, 1986 - ACS Publications
Positive Ion chemical ionization GC/MS was evaluated for the quantitation of
polychloroblphenyls (PCBs) using 10 or less selected PCB standards. Positive Ion chemical …

Analysis of polychlorinated biphenyls by quadrupole ion trap mass spectrometry: Part I—Chemical ionization studies of co-eluting congeners 77 and 110

M Lausevic, JB Plomley, X Jiang… - European Mass …, 1995 - journals.sagepub.com
A quadrupole ion trap mass spectrometer coupled with a gas chromatograph was used to
study the reactions of two co-eluting polychlorinated biphenyl (PCB) compounds, congener …

Automated procedures for mass spectrometric determination of polychlorinated biphenyls as isomer groups

LE Slivon, JE Gebhart, TL Hayes… - Analytical …, 1985 - ACS Publications
Software was developed to perform fully automated Identifi-cation and measurement of
polychlorinated biphenyls (PCBs) In environmental sample extracts analyzed with capillary …

Analysis of polychlorinated biphenyls by quadrupole ion trap mass spectrometry. Part II: Comparison of mass spectrometric detection using electron impact and …

M Lausević, X Jiang, RE March… - … in mass spectrometry, 1995 - Wiley Online Library
The responses of selected‐ion monitoring of electron impact mass spectra and selected‐
reagent‐ion chemical ionization mass spectra of polychlorinated biphenyls (PCBs), relative …

Analysis of the polychlorinated biphenyl problem. Application of gas chromatography-mass spectrometry with computer controlled repetitive data acquisition from …

JW Eichelberger, LE Harris, WL Budde - Analytical Chemistry, 1974 - ACS Publications
The polychlorinated biphenyls are a difficult-to-analyze class of environmental contaminants
because of the large number of possible individual isomers and their physical and chemical …

Mass spectrometric determination of polychlorinated biphenyls as isomer groups

JE Gebhart, TL Hayes, AL Alford-Stevens… - Analytical …, 1985 - ACS Publications
A procedure to measure concentrations of polychlorinated biphenyls (PCBs) by using nine
selected PCB congeners as concentration calibration standards was developed and ap …

Differentiation and characterization of isomeric polychlorinated biphenyls by gas-liquid chromatography coupled with electron impact and chemical ionization mass …

EO Oswald, L Levy, BJ Corbett, MP Walker - Journal of Chromatography A, 1974 - Elsevier
This report describes the utilization of gas-liquid chromatography coupled with chemical
ionization and electron impact mass spectrometry for the characterization and isomeric …

Rapid chromatography for the determination of polychlorinated biphenyls by GC-MS in environmental monitoring

AA Nikonova, AG Gorshkov - Analytical letters, 2011 - Taylor & Francis
A method for determination of polychlorinated biphenyls (PCBs) in environmental and
biological materials has been developed. This method includes rapid chromatography …

Chemical ionization mass spectrometry of specific polychlorinated biphenyl isomers

AG Harrison, FI Onuska, CW Tsang - Analytical Chemistry, 1981 - ACS Publications
The H2 and CH4 chemical ionization (Cl) mass spectra of selected polychlorinated biphenyl
isomers (PCBs) have been studied In detall. The H2 Cl mass spectra are shown to pro-vide …