Double role of polyethylene glycol in the microwaves-assisted non-hydrolytic synthesis of nanometric TiO2: oxygen source and stabilizing agent

D Morselli, M Niederberger, I Bilecka… - Journal of nanoparticle …, 2014 - Springer
The microwaves-assisted reaction between titanium (IV) tetrachloride and polyethylene
glycol (PEG) represents a novel non-aqueous sol–gel route for synthesizing surface …

Low temperature deposition of TiO2 layers from nanoparticle containing suspensions synthesized by microwave hydrothermal treatment

M Arin, J Watté, G Pollefeyt, K De Buysser… - Journal of sol-gel …, 2013 - Springer
In this paper, we present a microwave-assisted, hydrothermal method for the synthesis of
TiO 2 suspensions. These were obtained from Ti 4+ aqueous precursor solutions using …

Synthesis of nanocrystalline titania via microwave-assisted homogeneous hydrolysis under hydrothermal conditions

E A. Moskalenko, A A. Sadovnikov… - Current Microwave …, 2014 - benthamdirect.com
In this paper, we report on a new procedure for nanocrystalline titania synthesis using
microwave-assisted homogeneous hydrolysis under hydrothermal conditions. We show that …

Water-dispersible TiO2 nanoparticles via a biphasic solvothermal reaction method

R Mohan, J Drbohlavova, J Hubalek - Nanoscale research letters, 2013 - Springer
A biphasic solvothermal reaction method has been used for the synthesis of TiO 2
nanoparticles (NPs). In this method, hydrolysis and nucleation occur at the interface of …

[PDF][PDF] Effect of synthesis duration and HCl acid concentration on the formation of hydrothermally synthesised TiO2 nanoparticles

J Lind - 2015 - core.ac.uk
It is known when synthesising nanomaterial on laboratory scale, a variation in a single
synthesis parameter may alter the product. Numerous synthesis techniques have been …

Sol‐gel titanium dioxide nanoparticles: preparation and structural characterization

OL Kang, A Ahmad, UA Rana… - Journal of …, 2016 - Wiley Online Library
Titanium dioxide (TiO2) nanoparticle was achieved in an alternative sol‐gel route, as
involved in 1 M acidic solution: HCl‐tetrahydrofuran (HCl‐THF), HNO3‐tetrahydrofuran …

Chemical modification of titanium isopropoxide for producing stable dispersion of titania nano-particles

S Mahata, B Mondal, SS Mahata, K Usha… - Materials Chemistry and …, 2015 - Elsevier
Stable colloidal TiO 2 nano-particles are synthesized through the controlled hydrolysis of
chemically modified titanium (Ti) isopropoxide with acetylacetone and acetic acid whereas …

Preparation of water-dispersible TiO 2 nanoparticles from titanium tetrachloride using urea hydrogen peroxide as an oxygen donor

N Watanabe, T Kaneko, Y Uchimaru, S Yanagida… - …, 2013 - pubs.rsc.org
TiO2 nanoparticles were prepared from titanium tetrachloride (TiCl4) in CH2Cl2 at 80° C for
30 h, 42 h and 70 h using urea hydrogen peroxide (UHP) as an oxygen donor with a TiCl4 …

Large-surface mesoporous TiO2 nanoparticles: Synthesis, growth and photocatalytic performance

X Yang, H Fu, A Yu, X Jiang - Journal of colloid and interface science, 2012 - Elsevier
This study demonstrates a facile and effective method to generate mono-dispersed titanium
dioxide spheres at ambient conditions. The size of the colloids can be controlled from 60 to …

Microwave-Assisted Vacuum Synthesis of TiO2 Nanocrystalline Powders in One-Pot, One-Step Procedure

E Paradisi, R Rosa, G Baldi, V Dami, A Cioni, G Lorenzi… - Nanomaterials, 2021 - mdpi.com
A new method for fast and simple synthesis of crystalline TiO2 nanoparticles with
photocatalytic activity was developed by carrying out a classic sol–gel reaction directly …