Gas chromatographic and mass spectrometric determination of chlorophenoxy acids and related herbicides as their (cyanoethyl) dimethylsilyl derivatives

MJ Bertrand, AH Ahmed, B Sarrasin… - Analytical …, 1987 - ACS Publications
A method using (2-cyanoethyl) dlmethyl (dlethylamlno) sllane to form derivatives with
phenoxy acid herbicides and related compounds Is presented. Results obtained with 18 …

Gas-chromatographic analysis of insensitive pesticides as their halomethyldimethylsilyl derivatives

CA Bache, LE St. John, DJ Lisk - Analytical chemistry, 1968 - ACS Publications
The bromo-and chloromethyldimethylsilyl derivatives of acidic and phenolic pesticide and
herbicide compounds have been prepared which greatly enhance their responsewhen …

Novel derivatisation technique for the determination of chlorophenoxy acid type herbicides by gas chromatography–mass spectrometry

E Maloschik, M Mörtl, A Székács - Analytical and bioanalytical chemistry, 2010 - Springer
The analytical detection of chlorophenoxycarboxylic-acid-type herbicides (2, 4-D,
dichloprop, MCPA, etc.) in environmental samples is often a problem in instrumental …

Spectroscopic properties of the methyl esters of chlorophenoxy acid herbicides

CH Van Peteghem… - Journal of the Association …, 1975 - academic.oup.com
The mass and infrared spectra of the methyl esters of 9 chlorophenoxy acid herbicides are
presented. Ultraviolet data are discussed and proton magnetic resonance spectra are …

Determination of chlorophenoxy acids in formulations by gas-liquid chromatography of their trimethylsilyl derivatives

RH Collier, GS Grimes - Journal of the Association of Official …, 1974 - academic.oup.com
A rapid, precise, and specific method for the analysis of free acid and amine salt
formulations of chlorophenoxy acids has been developed. Samples containing the amine …

Gas chromatograph/mass spectrometer techniques for determination of interferences in pesticide analysis

EJ Bonelli - Analytical Chemistry, 1972 - ACS Publications
The electron capture detector has long been employedin the analysis of chlorinated
hydrocarbon pesticides. Its high sensitivity and excellent selectivity have made it the detector …

Determination of chlorophenoxy and other acidic herbicide residues in ground water by capillary gas chromatography of their alkyl esters formed by rapid …

S Butz, HJ Stan - Journal of Chromatography A, 1993 - Elsevier
A simple method for the determination of several chlorophenoxy acid and other acidic
herbicides as methyl, ethyl and butyl esters by means of capillary gas chromatography is …

Determination of chlorophenoxy acid herbicides by densitometry on thin layer chromatograms

J Sherma, J Koropchack - Analytica Chimica Acta, 1977 - Elsevier
A quantitative in situ tlc method for the determination of chlorophenoxy acid herbicides and
their salts in waters is described. The detection limit (1 ppb) is similar to that obtainable by …

Pentafluorobenzylation derivatization for determination of chlorinated herbicide acids

DF Gurka, FL Shore, ST Pan - Journal of the Association of …, 1987 - academic.oup.com
Pentafluorobenzyl and methyl esterification methods for several common herbicide acids
have been evaluated and compared. Gas chromatography,'electron capture instrumental …

Analysis of technical chlordane by gas chromatography/mass spectrometry

GW Sovocool, RG Lewis, RL Harless… - Analytical …, 1977 - ACS Publications
The composition of technical chlordane has been Investigated by combined gas
chromatography/mass spectrometry, em-ploying a column commonly used for pesticide …