Interlaboratory comparison of thermospray and particle beam liquid chromatography/mass spectrometry interfaces: evaluation of a chlorinated phenoxy acid herbicide …

TL Jones, LD Betowski, B Lesnik… - … science & technology, 1991 - ACS Publications
Seven laboratories participated in an interlaboratory evaluation of a liquid
chromatography/mass spectrometry (LC/MS) method for the analysis of 10 chlorinated …

Validation of liquid chromatography—mass spectrometry methods: interlaboratory studies

TL Jones, LD Betowski, V Lopez-Avila - TrAC Trends in Analytical …, 1994 - Elsevier
Developments over the last 15 years have led to widespread acceptance and
commercialization of two liquid chromatography—mass spectrometry (LC-MS) interfaces …

Evaluation of eluents in thermospray liquid chromatography-mass spectrometry for identification and determination of pesticides in environmental samples

D Barceló, G Durand, RJ Vreeken, GJ De Jong… - … of Chromatography A, 1991 - Elsevier
The influence of different eluents in positive and negative ion mode thermospray liquid
chromatography-mass spectrometry was studied with several groups of pesticides, including …

A comparison between positive and negative ion modes in thermospray liquid chromatography-mass spectrometry for the determination of chlorophenols and …

D Barceló - Chromatographia, 1988 - Springer
Positive and negative ion modes (Pl and NI, respectively) have been employed for the
characterization of 2, 4-dichlorophenol, 2, 4, 5-trichlorophenol, pentachlorophenol, Linuron …

Influence of reversed‐and normal‐phase liquid chromatographic eluents in the fragmentation of selected chlorinated herbicides in thermospray liquid chromatography …

D Barceló - Organic mass spectrometry, 1989 - Wiley Online Library
The effect of two completely different mobile phase compositions, reversed‐phase
acetonitrile‐water+ ammonium acetate and normal‐phase cyclohexane, were compared in …

Postcolumn addition of buffer for thermospray liquid chromatography/mass spectrometry identification of pesticides

RD Voyksner, JT Bursey, ED Pellizzari - Analytical Chemistry, 1984 - ACS Publications
Coaxial and right-angle tees were evaluated as methods of postcolumn buffer addition for
thermospray LC/MS analysis. The coaxial tee, which showed slightly better total Ion current …

Optimization and application of thermospray high-performance liquid chromatography/mass spectrometry

RD Voyksner, CA Haney - Analytical Chemistry, 1985 - ACS Publications
Thermospray (TSP) HPLC/MS frequently produces molecular weight Information and
exhibits lower detection limits than other HPLC/MS techniques for certain compounds …

Evidence for thermal decomposition contributions to the mass spectra of chlorinated phenoxyacid herbicides obtained by particle beam liquid chromatography mass …

LD Betowski, CM Pace, MR Roby - Journal of the American Society for …, 1992 - Elsevier
The spectral quality of a group of chlorinated phenoxyacid herbicides has been shown to
degrade under certain conditions upon introduction into the mass spectrometer by a particle …

New approach for the analysis of acidic pesticides in water by LC/MS with a particle beam interface

A Cappiello, G Famiglini, P Palma… - … science & technology, 1995 - ACS Publications
A new method for the determination of 18 acidic pesticides in water by liquid
chromatography/mass spectrometry is presented. A liquid-solid extrac-tion procedure for the …

Column liquid chromatography-mass spectrometry: selected techniques in environmental applications for polar pesticides and related compounds

J Slobodnik, BLM Van Baar, UAT Brinkman - Journal of chromatography A, 1995 - Elsevier
A review covering the field of environmental applications of liquid chromatography-mass
spectrometry (LC-MS) is presented. Recent developments and advances are discussed with …