Analysis of chlorophenoxy acid herbicides in water by large-volume on-line derivatization and gas chromatography–mass spectrometry

WH Ding, CH Liu, SP Yeh - Journal of chromatography A, 2000 - Elsevier
This work presents a modified method to analyze chlorophenoxy acid herbicides in water
samples. The herbicides 2, 4-D (2, 4-dichlorophenoxyacetic acid), Silvex (2, 4, 5 …

Determination of chlorophenoxy acid herbicides in water by in situ esterification followed by in-vial liquid–liquid extraction combined with large-volume on-column …

MI Catalina, J Dallüge, RJJ Vreuls, A Udo - Journal of chromatography A, 2000 - Elsevier
A new approach for rapidly analysing chlorophenoxy acid herbicides in water is presented.
The chlorinated acids are derivatised with dimethyl sulphate in the water sample itself (800 …

Chlorinated acid herbicides in water by strong anion-exchange disk extraction and in-vial elution and derivatization

JA Field, K Monohan - Journal of Chromatography A, 1996 - Elsevier
An analytical method for rapidly and quantitatively detecting chlorophenoxy acid herbicides
in water is presented. Strong anion-exchange, 25-mm diameter solid-phase extraction disks …

On-line preconcentration, cleanup and high-performance liquid chromatographic determination of chlorophenoxy acid herbicides in water

LE Vera-Avila, PC Padilla, MG Hernandez… - … of Chromatography A, 1996 - Elsevier
A rapid and simple technique for the determination of six chlorophenoxy acid herbicides in
water is described. After extraction and preconcentration of the analytes at pH≈ 1 in a small …

Determination of chlorophenoxy herbicides in waters by capillary gas chromatography with ion trap detection

ALS Pena, M Irene, N Silveira - Journal of Chromatography A, 1997 - Elsevier
A method for the determination of 4-chloro-2-methylphenoxyacetic acid (MCPA), 2, 4-
dichlorophenoxyacetic acid (2, 4-D) and 2, 4, 5-trichlorophenoxyacetic acid (2, 4, 5-T) in …

Rapid method for the determination of eight chlorophenoxy acid residues in environmental water samples using off-line solid-phase extraction and on-line selective …

JV Sancho-Llopis, F Hernandez-Hernandez… - Analytica chimica …, 1993 - Elsevier
A rapid procedure for the determination of eight chlorophenoxy acid herbicides in
environmental water samples is described. The method involves two off-line solid-phase …

Novel derivatisation technique for the determination of chlorophenoxy acid type herbicides by gas chromatography–mass spectrometry

E Maloschik, M Mörtl, A Székács - Analytical and bioanalytical chemistry, 2010 - Springer
The analytical detection of chlorophenoxycarboxylic-acid-type herbicides (2, 4-D,
dichloprop, MCPA, etc.) in environmental samples is often a problem in instrumental …

Determination of chlorophenoxy and other acidic herbicide residues in ground water by capillary gas chromatography of their alkyl esters formed by rapid …

S Butz, HJ Stan - Journal of Chromatography A, 1993 - Elsevier
A simple method for the determination of several chlorophenoxy acid and other acidic
herbicides as methyl, ethyl and butyl esters by means of capillary gas chromatography is …

Automated on-line in-tube solid-phase microextraction followed by liquid chromatography/electrospray ionization-mass spectrometry for the determination of …

M Takino, S Daishima, T Nakahara - Analyst, 2001 - pubs.rsc.org
A method for the determination of six chlorinated phenoxy acid herbicides in river water was
developed using in-tube solid-phase microextraction (SPME) followed by liquid …

Determination of phenoxyacid herbicides and their phenolic metabolites in surface and drinking water

S Marchese, D Perret, A Gentili… - … in mass spectrometry, 2002 - Wiley Online Library
An evaluation was made of the feasibility of using reversed‐phase liquid chromatography/
tandem mass spectrometry with an electrospray interface (LC/ESI‐MS/MS) to measure …