Development and validation of multi-residue analysis for tetracycline antibiotics in feed by high performance liquid chromatography coupled to mass spectrometry

E Patyra, K Kwiatek - Food Additives & Contaminants: Part A, 2017 - Taylor & Francis
ABSTRACT A new multi-residue method for the analysis of the tetracycline antibiotics
oxytetracycline, tetracycline, chlortetracycline, and doxycycline was developed and …

Comparison of HPLC–DAD and LC–MS techniques for the determination of tetracyclines in medicated feeds using one extraction protocol

E Patyra, K Kwiatek - Chromatographia, 2021 - Springer
Four antibiotics, oxytetracycline, tetracycline, doxycycline, and chlortetracycline were
separated and quantified in medicated feed. Tetracyclines from feed samples were extracted …

Analysis of tetracyclines in medicated feed for food animal production by HPLC-MS/MS

RE Gavilán, C Nebot, JM Miranda, Y Martín-Gómez… - Antibiotics, 2015 - mdpi.com
The use of medicated feed is a common practice in animal food production to improve
animal health. Tetracyclines and β-Lactams are the groups that are most frequently added to …

A Confirmatory Method Based on HPLC‐MS/MS for the Detection and Quantification of Residue of Tetracyclines in Nonmedicated Feed

RE Gavilán, C Nebot, M Veiga-Gómez… - Journal of Analytical …, 2016 - Wiley Online Library
The Commission Regulation 574/2011/EC set up maximum levels of coccidiostats and
histomonostats in nonmedicated feed as a consequence of carry‐over during …

[PDF][PDF] Analytical procedure for the determination of tetracyclines in medicated feedingstuffs by liquid chromatography-mass spectrometry

E Patyra, K Kwiatek - Journal of Veterinary Research, 2016 - sciendo.com
Introduction: The article presents a rapid and simple analytical procedure for determination
of four tetracyclines (oxytetracycline, tetracycline, chlortetracycline, and doxycycline) in …

Development and validation of an HPLC confirma‐tory method for the determination of tetracycline antibiotics residues in bovine muscle according to the European …

VF Samanidou, KI Nikolaidou… - Journal of separation …, 2005 - Wiley Online Library
A high‐performance liquid chromatographic method with diode‐array detection, at 351 nm,
was developed and validated for the determination of five tetracyclines (TCs): minocycline …

Determination of tetracycline antibiotics in animal tissues of food-producing animals by high-performance liquid chromatography using solid-phase extraction

J Sokol, E Matisova - Journal of Chromatography A, 1994 - Elsevier
A high-performance liquid chromatographic (HPLC) method was developed for the
determination of oxytetracycline (OTC), tetracycline (TC) and chlortetracycline (CTC) …

Determination of tetracyclines in pig and other meat samples using liquid chromatography coupled with diode array and tandem mass spectrometric detectors

Á Tölgyesi, L Tölgyesi, K Békési, VK Sharma, J Fekete - Meat science, 2014 - Elsevier
Two high performance liquid chromatographic methods (HPLC–DAD and LC–MS/MS) were
developed to analyze tetracycline (TC) residues in pig meat (pork) samples. The method …

Monitoring the presence of residues of tetracyclines in baby food samples by HPLC-MS/MS

C Nebot, M Guarddon, F Seco, A Iglesias, JM Miranda… - Food Control, 2014 - Elsevier
Tetracyclin is a group of antimicrobial permitted in animal food production, but their
concentrations in food of animal origin should not exceed 100 μg kg− 1 (in meat and milk) …

Development and validation method for the determination of selected tetracyclines in animal medicated feedingstuffs with the use of micellar liquid chromatography

E Patyra, E Kowalczyk, K Kwiatek - Analytical and bioanalytical chemistry, 2013 - Springer
A chromatographic procedure for the determination of oxytetracycline (OTC), tetracycline
(TC), chlorotetracycline (CTC), and doxycycline (DC) in medicated feedingstuffs was …