High-frequency dynamic nuclear polarization in the nuclear rotating frame

CT Farrar, DA Hall, GJ Gerfen, M Rosay… - Journal of Magnetic …, 2000 - Elsevier
A proton dynamic nuclear polarization (DNP) NMR signal enhancement (ϵ) close to thermal
equilibrium, ϵ= 0.89, has been obtained at high field (B0= 5 T, νepr= 139.5 GHz) using 15 …

Dynamic nuclear polarization using frequency modulation at 3.34 T

Y Hovav, A Feintuch, S Vega, D Goldfarb - Journal of Magnetic Resonance, 2014 - Elsevier
During dynamic nuclear polarization (DNP) experiments polarization is transferred from
unpaired electrons to their neighboring nuclear spins, resulting in dramatic enhancement of …

High frequency (140 GHz) dynamic nuclear polarization: polarization transfer to a solute in frozen aqueous solution

GJ Gerfen, LR Becerra, DA Hall, RG Griffin… - The Journal of …, 1995 - pubs.aip.org
Dynamic nuclear polarization (DNP) transfers the large polarization of unpaired electrons to
nuclei and thus significantly enhances the signal strength in nuclear magnetic resonance …

Inductively coupled NMR probe for versatile dynamic nuclear polarization operation at 7 T: Observation of 61±2% 1H polarization at 4 K

TA Siaw, SA Walker, BD Armstrong, SI Han - Journal of Magnetic …, 2012 - Elsevier
We have performed dynamic nuclear polarization (DNP) experiments at liquid helium
temperatures using a low-power (< 70mW) solid-state diode microwave source at 200GHz …

A spectrometer for dynamic nuclear polarization and electron paramagnetic resonance at high frequencies

LR Becerra, GJ Gerfen, BF Bellew, JA Bryant… - Journal of Magnetic …, 1995 - Elsevier
A high-frequency dynamic nuclear polarization (DNP)/electron paramagnetic resonance
spectrometer operating at 211 MHz for1H and 140 GHz forg= 2 paramagnetic centers (5 T …

Low-temperature dynamic nuclear polarization at 9.4 T with a 30 mW microwave source

KR Thurber, WM Yau, R Tycko - Journal of Magnetic Resonance, 2010 - Elsevier
Dynamic nuclear polarization (DNP) can provide large signal enhancements in nuclear
magnetic resonance (NMR) by transfer of polarization from electron spins to nuclear spins …

Dynamic nuclear polarization-enhanced 1H–13C double resonance NMR in static samples below 20 K

A Potapov, KR Thurber, WM Yau, R Tycko - Journal of Magnetic …, 2012 - Elsevier
We demonstrate the feasibility of one-dimensional and two-dimensional 1H–13C double
resonance NMR experiments with dynamic nuclear polarization (DNP) at 9.4 T and …

Dynamic nuclear polarization at 9 T using a novel 250 GHz gyrotron microwave source

VS Bajaj, CT Farrar, MK Hornstein, I Mastovsky… - Journal of Magnetic …, 2011 - Elsevier
In this communication, we report enhancements of nuclear spin polarization by dynamic
nuclear polarization (DNP) in static and spinning solids at a magnetic field strength of 9T …

[HTML][HTML] Dynamic nuclear polarization enhanced NMR at 187 GHz/284 MHz using an extended interaction Klystron amplifier

TF Kemp, HRW Dannatt, NS Barrow, A Watts… - Journal of Magnetic …, 2016 - Elsevier
Abstract A Dynamic Nuclear Polarisation (DNP) enhanced solid-state Magic Angle Spinning
(MAS) NMR spectrometer which uses a 187 GHz (corresponding to 1 H NMR frequency of …

High frequency dynamic nuclear polarization

QZ Ni, E Daviso, TV Can, E Markhasin… - Accounts of chemical …, 2013 - ACS Publications
During the three decades 1980–2010, magic angle spinning (MAS) NMR developed into the
method of choice to examine many chemical, physical, and biological problems. In …