Study of blood collection and sample preparation for analysis of vitamin D and its metabolites by liquid chromatography–tandem mass spectrometry

A Mena-Bravo, F Priego-Capote, MDL de Castro - Analytica Chimica Acta, 2015 - Elsevier
The analysis of vitamin D status, with special emphasis on 25-hydroxyvitamin D and 1, 25-
dihydroxyvitamin D, is gaining interest in clinical studies due to the classical and non …

Quantitative analytical method to evaluate the metabolism of vitamin D

A Mena-Bravo, C Ferreiro-Vera, F Priego-Capote… - Clinica chimica acta, 2015 - Elsevier
A method for quantitative analysis of vitamin D (both D 2 and D 3) and its main metabolites—
monohydroxylated vitamin D (25-hydroxyvitamin D 2 and 25-hydroxyvitamin D 3) and …

Determination of vitamin D3 metabolites: state-of-the-art and trends

MDL de Castro, JM Fernández-Romero… - … of pharmaceutical and …, 1999 - Elsevier
The steps involved in the methods for the determination of vitamin D3 metabolites (namely,
25-hydroxyvitamin D3, 1, 25-dihydroxyvitamin D3, 24, 25-dihydroxyvitamin D3) mainly in …

Improved sample preparation method for fast LC-MS/MS analysis of vitamin D metabolites in serum

R Rola, K Kowalski, T Bieńkowski… - Journal of Pharmaceutical …, 2020 - Elsevier
Despite the fact that more than 90% of vitamin D analysis are performed using immuno-
enzymatic techniques, it is liquid chromatography coupled with tandem mass spectrometry …

Overview of extraction methods for analysis of vitamin D and its metabolites in biological samples

ML Musteata, FM Musteata - Bioanalysis, 2011 - Taylor & Francis
In the last decade the scientific and medical community was confronted with a renewed
interest in vitamin D and its metabolites, interest prompted by new discoveries regarding the …

Simultaneous quantification of four vitamin D metabolites in human serum using high performance liquid chromatography tandem mass spectrometry for vitamin D …

S Baecher, A Leinenbach, JA Wright, S Pongratz… - Clinical …, 2012 - Elsevier
OBJECTIVES: For quantification of 25-hydroxyvitamin D3 (25OH-D3), 25-hydroxyvitamin D2
(25OH-D2), 3-epi-25-hydroxyvitamin D3 (3-epi-25OH-D3) and 24R, 25-dihydroxyvitamin D3 …

Liquid chromatography–mass spectrometric method combined with derivatization for determination of 1α-hydroxyvitamin D3 in human plasma

T Higashi, D Awada, K Shimada - Journal of Chromatography B, 2002 - Elsevier
A stable isotope dilution liquid chromatography–tandem mass spectrometric (LC–MS–MS)
method for the determination of plasma 1α-hydroxyvitamin D3 [1α (OH) D3] has been …

Determination of 25‐hydroxyvitamin D3 in human plasma using HPLC with UV detection based on SPE sample preparation

R Kand'ár, P Žáková - Journal of separation science, 2009 - Wiley Online Library
Interest in the metabolism and physiological action of vitamin D is increased exponentially.
The most important metabolites of vitamin D are 25‐hydroxyvitamin and 1, 25 …

HPLC determination of Vitamin D3 and its metabolite in human plasma with on-line sample cleanup

MR Brunetto, MA Obando, M Gallignani, OM Alarcón… - Talanta, 2004 - Elsevier
A HPLC method with automated column switching and UV-diode array detection is
described for the simultaneous determination of Vitamin D3 and 25-hydroxyvitamin D3 (25 …

Vitamin D analysis in plasma by high performance liquid chromatography (HPLC) with C30 reversed phase column and UV detection–easy and acetonitrile-free

L Hymøller, SK Jensen - Journal of Chromatography a, 2011 - Elsevier
Two physiologically important forms of vitamin D exist: vitamin D2 and vitamin D3, which by
liver based hydroxylase enzymes are converted to 25-hydroxyvitamin D2 and 25 …