Characterization of the thermal decomposition products of the sulfonylurea herbicide chlorsulfuron

AR Long, B Charkhian, LC Hsieh, CR Short… - … of Chromatography A, 1990 - Elsevier
Gas chromatography injection port thermal decomposition of chlorsulfuron resulted in two
volatile decomposition products (2-amino-4-methoxy-6-methyl-1, 3, 5-triazine and 2 …

Analysis of sulfonylurea herbicides by gas-liquid chromatography. 1. Formation of thermostable derivatives of chlorsulfuron and metsulfuron-methyl

P Klaffenbach, PT Holland… - Journal of agricultural and …, 1993 - ACS Publications
A method is described to overcome the thermalinstability of sulfonylurea herbicides and thus
enable their analysis by gas chromatography (GC). Methylationof chlorsulfuron by …

Analysis of sulfonylurea herbicides by gas-liquid chromatography. 2. Determination of chlorsulfuron and metsulfuron-methyl in soil and water samples

P Klaffenbach, PT Holland - Journal of Agricultural and Food …, 1993 - ACS Publications
Sulfonylureas are extracted from water samples using solid-phase extraction (SPE) with Cl8-
silica/Teflon disks. Soil samples are extracted with 0.1 M sodium hydrogen carbonate, and …

Pyrolysis—gas chromatography/mass spectrometry and electron impact-, fast atom bombardment-mass spectrometry of sulfonylureas

GC Galletti, G Chiavari, FA Mellon, K Parlsey - Journal of analytical and …, 1991 - Elsevier
Four sulfonylurea herbicides, ie chlorsulfuron, metsulfuron methyl, thiameturon methyl and
chlorimuron ethyl, were analyzed by pyrolysis-gas chromatography/mass spectrometry (Py …

Analysis of sulfonylurea herbicides by gas–liquid chromatography III—mass spectrometry and multiresidue determination

P Klaffenbach, PT Holland - Biological mass spectrometry, 1993 - Wiley Online Library
A method is described for the determination of sulfonylurea herbicides by gas
chromatography (GC). Chlorimuronethyl, cinosulfuron, primisulfuron‐methyl, thifensulfuron …

Liquid chromatography/mass spectrometry of the thermally labile herbicides, chlorsulfuron and sulfometuron methyl

LM Shalaby - Biomedical mass spectrometry, 1985 - Wiley Online Library
An on‐line liquid chromatographic/mass spectrometric technique with direct liquid
introduction (DLI) was investigated for the analysis of chlorsulfuron, the active ingredient of …

Investigation of selected sulfonylurea herbicides by TLC and HPLC

M Miszczyk, A Pyka - Journal of liquid chromatography & related …, 2006 - Taylor & Francis
The following selected sulfonylurea herbicides have been investigated: thifensulfuron
methyl (10), triasulfuron (11), chlorsulfuron (12), rimsulfuron (13), amidosulfuron (14), and …

Capillary column gas chromatographic determination of trace residues of the herbicide chlorsulfuron in agricultural runoff water

U Ahmad - Journal of the Association of Official Analytical …, 1987 - academic.oup.com
A capillary column gas chromatographic method is described for determining parts-per-
trillion (ppt) levels of chlorsulfuron in agricultural runoff water. The water sample is acidified …

Application of thermospray LC/MS for residue analysis of sulfonylurea herbicides and their degradation products

LM Shalaby, FQ Bramble, PW Lee - Journal of Agricultural and …, 1992 - ACS Publications
MATERIALS AND METHODS Chemicals. Analytical standards (> 99% pure) for nicosulf-
uron, rimriduron, and the two metabolites were synthesized at the Experimental Station (Du …

Determination of the sulfonylurea herbicides chlorsulfuron and metsulfuron‐methyl in soil, water and plant material by gas chromatography of their pentafluorobenzyl …

EG Cotterill - Pesticide science, 1992 - Wiley Online Library
The measurement of the sulfonyl urea herbicides, chlorsulfuron and metsulfuron‐methyl as
pentafluorobenzyl derivatives has been investigated and the kinetics of reaction optimised …