An integrated approach to polymer reaction engineering: a review of calorimetry and state estimation

TF Mckenna, S Othman, G Fevotte… - Polymer Reaction …, 2000 - Taylor & Francis
In order to completely master a polymerisation process, it is necessary to take a pluri-
disciplinary approach that incorporates the use of kinetic and polymer property models (eg …

On-line monitoring of emulsion copolymerisations using hardware sensors and calorimetry

P Guinot, N Othman, G Févotte… - Polymer Reaction …, 2000 - Taylor & Francis
We have used a simplified model of emulsion polymerisation, along with an adaptive
calorimetric approach and a set of non-linear state estimators to monitor the individual …

Computer-aided parameter estimation and on-line monitoring of emulsion and solution polymerisation reactors

G Fevotte, I Barudio, TF McKenna - Computers & chemical engineering, 1996 - Elsevier
The production of polymers is a complex process that produces material of which the quality
is highly sensitive to operating conditions. Much work has been done in the past on the …

Polymer reaction engineering: from reaction kinetics to polymer reactor control

A Penlidis - The Canadian Journal of Chemical Engineering, 1994 - Wiley Online Library
Polymer reaction engineering is a relatively “young”, very broad, multidisciplinary, rapidly
developing field. It is the combination of polymer science, chemistry and technology with …

Control of polymerization reactors

JR Leiza, JC Pinto - Polymer Reation Engineering, 2008 - Wiley Online Library
Monitoring of polymerization variables is necessary to fully implement advanced closedloop
control strategies and to ensure the consistent, safe and optimal production of polymeric …

[图书][B] Handbook of polymer reaction engineering

T Meyer, JTF Keurentjes - 2005 - research.tue.nl
This first book dedicated to all aspects of the field presents our current knowledge in its
entirety, covering the necessary disciplines and processes involved-from the monomer to …

On-line monitoring and modelling of free radical copolymerisations: Butyl Acrylate/Vinyl Acetate

S Othman, I Barudio, G Fevotte… - Polymer Reaction …, 1999 - Taylor & Francis
After demonstrating the efficiency of a previously-developed method for the estimation of the
rate of heat generation in a stirred tank polymerisation reactor, the use of a non-linear state …

Online reaction calorimetry. Applications to the monitoring of emulsion polymerization without samples or models of the heat-transfer coefficient

S BenAmor, D Colombié… - Industrial & engineering …, 2002 - ACS Publications
A high-gain nonlinear cascade state estimator is presented in this work and used to monitor
conversion and polymer composition in an emulsion copolymerization process. The …

Measurement and control of polymerization reactors

JR Richards, JP Congalidis - Computers & chemical engineering, 2006 - Elsevier
The measurement and control of polymerization reactors is very challenging due to the
complexity of the physical mechanisms and polymerization kinetics. In these reactors many …

Calorimetric estimation for a batch-loop emulsion polymerisation reactor

S Fan, E Alpay - Chemical engineering science, 2004 - Elsevier
To facilitate the online monitoring and control of a pilot-scale polymerisation reactor, state
estimation techniques are investigated. Specifically, a batch-loop reactor is employed for the …