Crystallographic evidence of a base-free uranium (IV) terminal oxo species
SJ Kraft, J Walensky, PE Fanwick, MB Hall… - Inorganic …, 2010 - ACS Publications
Inorganic chemistry, 2010•ACS Publications
The uranium (IV) terminal oxo species Tp* 2U (O) has been synthesized by oxygen-atom
transfer from pyridine-N-oxide to Tp* 2U (2, 2′-bipyridine), a trivalent uranium species with
a monoanionic bipyridine ligand. Full characterization of the oxo species using 1H NMR and
IR spectroscopies, X-ray crystallography, and computational studies was performed.
transfer from pyridine-N-oxide to Tp* 2U (2, 2′-bipyridine), a trivalent uranium species with
a monoanionic bipyridine ligand. Full characterization of the oxo species using 1H NMR and
IR spectroscopies, X-ray crystallography, and computational studies was performed.
The uranium(IV) terminal oxo species Tp*2U(O) has been synthesized by oxygen-atom transfer from pyridine-N-oxide to Tp*2U(2,2′-bipyridine), a trivalent uranium species with a monoanionic bipyridine ligand. Full characterization of the oxo species using 1H NMR and IR spectroscopies, X-ray crystallography, and computational studies was performed.
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