Determination of 129I using volatilization method and liquid scintillation spectrometry
B Remenec, S Dulanská, B Horváthová… - Journal of Radioanalytical …, 2017 - Springer
B Remenec, S Dulanská, B Horváthová, Ľ Mátel
Journal of Radioanalytical and Nuclear Chemistry, 2017•SpringerA simple and rapid separation method for 129 I determination in radioactive waste samples
was developed. Suitable conditions for iodine volatilization were tested. Iodine was trapped
in 1.5 mol L− 1 NaOH and precipitated as PdI 2· H 2 O by addition of PdCl 2 with recoveries
higher than 80%. The method was applied for analysis of contaminated soil, radioactive
sludge, evaporator concentrate and heterogeneous waste samples from nuclear power
plants in Slovak Republic. 129 I was measured on liquid scintillation counter TRI CARB …
was developed. Suitable conditions for iodine volatilization were tested. Iodine was trapped
in 1.5 mol L− 1 NaOH and precipitated as PdI 2· H 2 O by addition of PdCl 2 with recoveries
higher than 80%. The method was applied for analysis of contaminated soil, radioactive
sludge, evaporator concentrate and heterogeneous waste samples from nuclear power
plants in Slovak Republic. 129 I was measured on liquid scintillation counter TRI CARB …
Abstract
A simple and rapid separation method for 129I determination in radioactive waste samples was developed. Suitable conditions for iodine volatilization were tested. Iodine was trapped in 1.5 mol L−1 NaOH and precipitated as PdI2·H2O by addition of PdCl2 with recoveries higher than 80%. The method was applied for analysis of contaminated soil, radioactive sludge, evaporator concentrate and heterogeneous waste samples from nuclear power plants in Slovak Republic. 129I was measured on liquid scintillation counter TRI CARB 2900 TR using Ultima Gold AB scintillation cocktail.
Springer
以上显示的是最相近的搜索结果。 查看全部搜索结果