Expanding the Dimensions of a Small, Two-Dimensional Diffraction Detector

X Chen, MR Hauwiller, A Kumar… - Microscopy and …, 2020 - academic.oup.com
Microscopy and Microanalysis, 2020academic.oup.com
We report an approach to expand the effective number of pixels available to small, two-
dimensional electron detectors. To do so, we acquire subsections of a diffraction pattern that
are then accurately stitched together in post-processing. Using an electron microscopy pixel
array detector (EMPAD) that has only 128× 128 pixels, we show that the field of view can be
expanded while achieving high reciprocal-space sampling. Further, we highlight the need to
properly account for the detector position (rotation) and the non-orthonormal diffraction shift …
Abstract
We report an approach to expand the effective number of pixels available to small, two-dimensional electron detectors. To do so, we acquire subsections of a diffraction pattern that are then accurately stitched together in post-processing. Using an electron microscopy pixel array detector (EMPAD) that has only 128 × 128 pixels, we show that the field of view can be expanded while achieving high reciprocal-space sampling. Further, we highlight the need to properly account for the detector position (rotation) and the non-orthonormal diffraction shift axes to achieve an accurate reconstruction. Applying the method, we provide examples of spot and convergent beam diffraction patterns acquired with a pixelated detector.
Oxford University Press
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