Generation of lanthanide coordination polymers with dicarboxylate ligands: synthesis, structure, thermal decomposition and magnetic properties of the two …
M Hernández-Molina, PA Lorenzo-Luis, T López… - …, 2000 - pubs.rsc.org
CrystEngComm, 2000•pubs.rsc.org
The malonate complex of formula [Pr2 (C3H2O4) 3 (H2O) 3]· 2H2O (1) was prepared and
his crystal structure determined by X-ray diffraction methods. 1 crystallizes in the monoclinic
space group P21, Z= 4, with unit cell parameters a= 7.631 (2), b= 12.899 (4), c= 8.923 (2) Å
and β= 101.11 (3)°. 1 is a polymer which grows in the (110) plane. The hydrogen bond
stabilizes the crystal structure forming a three-dimensional network. The two non-equivalent
praseodymium (III) ions have different environments. Finally, the thermal behaviour and …
his crystal structure determined by X-ray diffraction methods. 1 crystallizes in the monoclinic
space group P21, Z= 4, with unit cell parameters a= 7.631 (2), b= 12.899 (4), c= 8.923 (2) Å
and β= 101.11 (3)°. 1 is a polymer which grows in the (110) plane. The hydrogen bond
stabilizes the crystal structure forming a three-dimensional network. The two non-equivalent
praseodymium (III) ions have different environments. Finally, the thermal behaviour and …
The malonate complex of formula [Pr2(C3H2O4)3(H2O)3]·2H2O (1) was prepared and his crystal structure determined by X-ray diffraction methods. 1 crystallizes in the monoclinic space group P21, Z = 4, with unit cell parameters a = 7.631(2), b = 12.899(4), c = 8.923(2) Å and β = 101.11(3)°. 1 is a polymer which grows in the (110) plane. The hydrogen bond stabilizes the crystal structure forming a three-dimensional network. The two non-equivalent praseodymium(III) ions have different environments. Finally, the thermal behaviour and magnetic properties were investigated.
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