Growth and vibrational spectroscopy of K2LiyNixCo1-xSO42. 6H2O (y= 0.1; 0.2; 0.3; 0.4) crystals
TS Pacheco, ZMC Ludwig, DR Sant'Anna… - Vibrational …, 2020 - Elsevier
The mixed crystals of the Tutton's salt doped with Li following the empirical formula K 2 Li y
Ni x Co 1-x (SO 4) 2. 6H 2 O, were synthesized from the slow evaporation of the solvent at
constant temperature. The presence of K, S, Ni, Co and O elements in the studied crystalline
structure was confirmed by EDS spectroscopy using a scanning electron microscope and
their quantification including Li was carried out with the help of ICP-OES technique. Raman
spectroscopy in the range 100− 3600 cm− 1, confirmed the presence of tetrahedral (SO 4) …
Ni x Co 1-x (SO 4) 2. 6H 2 O, were synthesized from the slow evaporation of the solvent at
constant temperature. The presence of K, S, Ni, Co and O elements in the studied crystalline
structure was confirmed by EDS spectroscopy using a scanning electron microscope and
their quantification including Li was carried out with the help of ICP-OES technique. Raman
spectroscopy in the range 100− 3600 cm− 1, confirmed the presence of tetrahedral (SO 4) …
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