Investigation on the growth of DAST crystals of large surface area for THz applications
Materials Chemistry and Physics, 2012•Elsevier
The growth of high quality 4-N, N-dimethylamino-4-N-methyl-stilbazoliumtosylate (DAST)
crystal with large surface area is reported by adopting the slope nucleation coupled slow
evaporation method (SNM-SE). The structure and composition of the crystal are studied by
single crystal X-ray diffraction and CHN analyses. The linear optical properties are
investigated by UV–vis absorption. The melting point and thermal behavior of DAST are
investigated using differential scanning calorimetric (DSC) and thermogravimetric analyses …
crystal with large surface area is reported by adopting the slope nucleation coupled slow
evaporation method (SNM-SE). The structure and composition of the crystal are studied by
single crystal X-ray diffraction and CHN analyses. The linear optical properties are
investigated by UV–vis absorption. The melting point and thermal behavior of DAST are
investigated using differential scanning calorimetric (DSC) and thermogravimetric analyses …
The growth of high quality 4-N,N-dimethylamino-4-N-methyl-stilbazoliumtosylate (DAST) crystal with large surface area is reported by adopting the slope nucleation coupled slow evaporation method (SNM-SE). The structure and composition of the crystal are studied by single crystal X-ray diffraction and CHN analyses. The linear optical properties are investigated by UV–vis absorption. The melting point and thermal behavior of DAST are investigated using differential scanning calorimetric (DSC) and thermogravimetric analyses (TGA). The Vickers microhardness number (VHN) and work hardening coefficient of the grown crystal have been determined. The surface features of the DAST crystal are analyzed by scanning electron microscopy (SEM) and it confirmed the presence of narrow line defects (NLDs) in the sample.
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