Polyindole-ZnO nanocomposite: synthesis, characterization and heterogeneous catalyst for the 3, 4-dihydropyrimidinone synthesis under solvent-free conditions

KN Handore, SV Bhavsar, N Pande… - Polymer-Plastics …, 2014 - Taylor & Francis
KN Handore, SV Bhavsar, N Pande, PK Chhattise, SB Sharma, S Dallavalle, V Gaikwad…
Polymer-Plastics Technology and Engineering, 2014Taylor & Francis
A Polyindole-ZnO nanocomposite particle was synthesized by using a chemical oxidative
polymerization method. Synthesized nanocomposite was characterized by UV-Visible, FTIR,
SEM, XRD, EDAX and electrical conductivity measurements. The band at∼ 3400 cm− 1 and
735 cm− 1 in FTIR spectra confirmed the polyindole formation. XRD spectral studies exhibits
major diffraction in between 30–40°(2θ) indicates the partial crystalline nature of the
polyindole-ZnO nanocomposite. SEM image reveals agglomerated granular particulate …
A Polyindole-ZnO nanocomposite particle was synthesized by using a chemical oxidative polymerization method. Synthesized nanocomposite was characterized by UV-Visible, FTIR, SEM, XRD, EDAX and electrical conductivity measurements. The band at ∼3400 cm−1 and 735 cm−1 in FTIR spectra confirmed the polyindole formation. XRD spectral studies exhibits major diffraction in between 30–40° (2θ) indicates the partial crystalline nature of the polyindole-ZnO nanocomposite. SEM image reveals agglomerated granular particulate nature with ZnO embedded in the polyindole matrix. The application of Polyindole-ZnO nanocomposite as a polymer-supported catalyst was studied for the synthesis of one pot multicomponent Biginelli condensation.
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