Spark plasma sintering and porosity studies of uranium nitride

KD Johnson, J Wallenius, M Jolkkonen… - Journal of Nuclear …, 2016 - Elsevier
KD Johnson, J Wallenius, M Jolkkonen, A Claisse
Journal of Nuclear Materials, 2016Elsevier
In this study, a number of samples of UN sintered by the SPS method have been fabricated,
and highly pure samples ranging in density from 68% to 99.8% TD–corresponding to an
absolute density of 14.25 g/cm 3 out of a theoretical density of 14.28 g/cm 3–have been
fabricated. By careful adjustment of the sintering parameters of temperature and applied
pressure, the production of pellets of specific porosity may now be achieved between these
ranges. The pore closure behaviour of the material has also been documented and …
Abstract
In this study, a number of samples of UN sintered by the SPS method have been fabricated, and highly pure samples ranging in density from 68% to 99.8%TD – corresponding to an absolute density of 14.25 g/cm3 out of a theoretical density of 14.28 g/cm3 – have been fabricated. By careful adjustment of the sintering parameters of temperature and applied pressure, the production of pellets of specific porosity may now be achieved between these ranges. The pore closure behaviour of the material has also been documented and compared to previous studies of similar materials, which demonstrates that full pore closure using these methods occurs near 97.5% of relative density.
Elsevier
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