Structural changes of tempered martensitic 9% Cr–2% W–3% Co steel during creep at 650 C

N Dudova, A Plotnikova, D Molodov, A Belyakov… - Materials Science and …, 2012 - Elsevier
N Dudova, A Plotnikova, D Molodov, A Belyakov, R Kaibyshev
Materials Science and Engineering: A, 2012Elsevier
The structural changes in tempered martensitic 9Cr–2W–3Co (wt%) steel during creep tests
at 650° C were studied. The starting material was a solution treated at 1050° C and
subsequently tempered at 750° C. The tempered martensite substructure consisted of a
mixture of crystallites with a lath-type morphology and equiaxed subgrains. The tempering
resulted in the precipitation of numerous second phase particles. MX-type precipitates were
homogeneously distributed within the ferritic matrix, whereas M23C6-type carbides were …
The structural changes in tempered martensitic 9Cr–2W–3Co (wt%) steel during creep tests at 650°C were studied. The starting material was a solution treated at 1050°C and subsequently tempered at 750°C. The tempered martensite substructure consisted of a mixture of crystallites with a lath-type morphology and equiaxed subgrains. The tempering resulted in the precipitation of numerous second phase particles. MX-type precipitates were homogeneously distributed within the ferritic matrix, whereas M23C6-type carbides were located on boundaries. Under creep conditions, Laves phase particles also precipitated at (sub)grain/lath boundaries. Laths and subgrains tended to coarsen during creep. It was shown that M23C6-type carbides played a major role in the stabilization of the tempered martensite lath structure by exerting a large pinning pressure. The transition to tertiary creep correlated with a coarsening of the carbides and a detachment of lath and subgrain boundaries from the chains of these carbides that led to a decreased pinning force from M23C6 carbides.
Elsevier
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