Synthesis of dimethylcyclosiloxanes in the active medium
AA Kalinina, EV Talalaeva, AI Demchenko… - Russian Chemical …, 2016 - Springer
AA Kalinina, EV Talalaeva, AI Demchenko, NG Vasilenko, YA Molodtsova, NV Demchenko…
Russian Chemical Bulletin, 2016•SpringerThe process of condensation of dimethyldiethoxysilane in the active medium in a presence
of acetyl chloride, trifluoroacetic acid, and sulfocationites has been investigated. Their
impact on the rate and selectivity of the process has been estimated. The prospects of the
application of sulfocationites for the polycondensation of dimethyldiethoxysilane in
anhydrous acetic acid with an 99% yield have been demonstrated.
of acetyl chloride, trifluoroacetic acid, and sulfocationites has been investigated. Their
impact on the rate and selectivity of the process has been estimated. The prospects of the
application of sulfocationites for the polycondensation of dimethyldiethoxysilane in
anhydrous acetic acid with an 99% yield have been demonstrated.
Abstract
The process of condensation of dimethyldiethoxysilane in the active medium in a presence of acetyl chloride, trifluoroacetic acid, and sulfocationites has been investigated. Their impact on the rate and selectivity of the process has been estimated. The prospects of the application of sulfocationites for the polycondensation of dimethyldiethoxysilane in anhydrous acetic acid with an 99% yield have been demonstrated.
Springer
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