In situ investigation on the evolution mechanism of heterogeneous micro-scale structure in potassium-niobate microwave flash sintering

Y Lu, X Yu, Y Wang, X Hu, F Xu - Scripta Materialia, 2024 - Elsevier
Heterogeneity in the final product of flash sintering is a significant limitation for massive
development. Synchrotron radiation computed tomography (SR-CT) was initially used to …

Induced internal stresses and their relation to FLASH sintering of KNN ceramics

R Serrazina, M Gomes, R Vilarinho, L Pereira… - Journal of Materials …, 2022 - pubs.rsc.org
Electric field and current applied to an unsintered ceramic body are known to promote low
temperature and extremely fast densification, in a process referred to as FLASH sintering …

[HTML][HTML] Particle characteristics' influence on FLASH sintering of potassium sodium niobate: A relationship with conduction mechanisms

R Serrazina, C Ribeiro, ME Costa, L Pereira… - Materials, 2021 - mdpi.com
The considerable decrease in temperature and time makes FLASH sintering a more
sustainable alternative for materials processing. FLASH also becomes relevant if volatile …

[HTML][HTML] Atmosphere-Assisted FLASH Sintering of Nanometric Potassium Sodium Niobate

R Serrazina, L Pereira, PM Vilarinho, AM Senos - Nanomaterials, 2022 - mdpi.com
The request for extremely low-temperature and short-time sintering techniques has guided
the development of alternative ceramic processing. Atmosphere-assisted FLASH sintering …

The role of particle contact in densification of FLASH sintered potassium sodium niobate

R Serrazina, AMOR Senos, L Pereira… - European Journal of …, 2020 - Wiley Online Library
Potassium sodium niobate, K0. 5Na0. 5NbO3 (KNN) is a lead‐free piezoelectric with the
potential to replace lead zirconate titanate (PZT) in electromechanical applications. Due to …

Modelling the particle contact influence on the Joule heating and temperature distribution during FLASH sintering

R Serrazina, PM Vilarinho, AMOR Senos… - Journal of the European …, 2020 - Elsevier
FLASH sintering is a field-assisted technique that allows the densification of ceramics in a
few seconds at temperatures significantly lower than those of conventional cycles. There is …

Real‐time capturing of microscale events controlling the sintering of lead‐free piezoelectric potassium‐sodium niobate

M Bah, R Podor, R Retoux, F Delorme, K Nadaud… - Small, 2022 - Wiley Online Library
Sintering is a very important process in materials science and technological applications.
Despite breakthroughs in achieving optimized piezoelectric properties, fundamentals of K0 …

Microwave flash sintering of metal powders: From experimental evidence to multiphysics simulation

C Manière, G Lee, T Zahrah, EA Olevsky - Acta Materialia, 2018 - Elsevier
Flash sintering phenomena are predominantly associated with ceramics due to thermal
runaway of their electric conductivity noticeably represented in materials such as zirconia or …

Fast-fired, nanograined titanium niobate (TiNb2O7) with enhanced dielectric properties

GS Falk, TB Wermuth, JBR Neto, SYG González… - Materials Science and …, 2020 - Elsevier
The interfacial polarization, the degree of densification and the grain size are factors that
directly influence the materials dielectric properties. This investigation show that is possible …

[HTML][HTML] Discussion on Microwave-Matter Interaction Mechanisms by In Situ Observation of “Core-Shell” Microstructure during Microwave Sintering

W Liu, F Xu, Y Li, X Hu, B Dong, Y Xiao - Materials, 2016 - mdpi.com
This research aims to deepen the understanding of the interaction mechanisms between
microwave and matter in a metal-ceramic system based on in situ synchrotron radiation …