Determination of barbiturates in biological specimens by flat membrane-based liquid-phase microextraction and liquid chromatography-mass spectrometry

R Zhu, Y Dong, X Cai, C Huang - Molecules, 2019 - mdpi.com
The wide abuse of barbiturates has aroused extensive public concern. Therefore, the
determination of such drugs is becoming essential in therapeutic drug monitoring and …

Simultaneous determination of barbiturates in human biological fluids by direct immersion solid-phase microextraction and gas chromatography–mass spectrometry

M Iwai, H Hattori, T Arinobu, A Ishii, T Kumazawa… - … of Chromatography B, 2004 - Elsevier
Simultaneous determination of seven barbiturates in human whole blood and urine by
combining direct immersion solid-phase microextraction (DI–SPME) with gas …

Determination of barbiturates by solid-phase microextraction (SPME) and ion trap gas chromatography–mass spectrometry

BJ Hall, JS Brodbelt - Journal of Chromatography A, 1997 - Elsevier
Solid-phase microextraction (SPME) in conjunction with quadrupole ion trap GC–MS was
applied to the determination of a series of barbiturates. A 65 μm Carbowax–divinylbenzene …

Rapid identification and quantitation of barbiturates in plasma using solid-phase extraction combined with GC-FID and GC-MS method

FH Qiu, L Liu, L Guo, Y Luo, YQ Lu - Yao xue xue bao= Acta …, 1995 - europepmc.org
A rapid screening method for the quantitation and identification of 7 barbiturates in plasma is
presented. The method employs solid-phase extraction at pH 3 using X-5 resin as …

Ultrasensitive enantiomeric barbiturate analysis in body fluids through capillary electrophoresis with large-volume sample stacking and ultrasound-assisted dispersive …

MC Chen, MM Hsieh, XY Huang - Journal of Chromatography A, 2024 - Elsevier
A rapid, straightforward, and sensitive approach to quantifying enantiomeric barbiturates in
serum was developed by integrating ultrasound-assisted dispersive liquid–liquid …

Development of a dispersive liquid–liquid microextraction method for spectrophotometric determination of barbituric acid in pharmaceutical formulation and biological …

AR Zarei, F Gholamian - Analytical biochemistry, 2011 - Elsevier
In this paper, a novel and simple method for the determination of trace amounts of barbituric
acid in water and biological samples was developed by using dispersive liquid–liquid …

Development of electrically assisted solvent bar microextraction followed by high performance liquid chromatography for the extraction and quantification of basic …

M Maghsoudi, S Nojavan, E Hatami - Journal of Chromatography A, 2021 - Elsevier
In this study, a new extraction procedure is introduced based on electrically assisted solvent
bar microextraction. In the first step, the analytes are transferred from sample solution to the …

Hollow‐fiber liquid‐phase microextraction and gas chromatography‐mass spectrometry of barbiturates in whole blood samples

RA Menck, DS De Lima, SC Seulin… - Journal of …, 2012 - Wiley Online Library
Here, we present a method for measuring barbiturates (butalbital, secobarbital,
pentobarbital, and phenobarbital) in whole blood samples. To accomplish these …

Comparison of hollow fiber liquid-phase microextraction and ultrasound-assisted low-density solvent dispersive liquid–liquid microextraction for the determination of …

L Meng, W Zhang, P Meng, B Zhu, K Zheng - Journal of Chromatography B, 2015 - Elsevier
Two microextraction techniques based on hollow fiber liquid-phase microextraction (HF-
LPME) and ultrasound-assisted low-density solvent dispersive liquid–liquid microextraction …

Extraction and preconcentration of β-blockers in human urine for analysis with high performance liquid chromatography by means of carrier-mediated liquid phase …

L Zhang, X Su, C Zhang, L Ouyang, Q Xie, M Ma, S Yao - Talanta, 2010 - Elsevier
A novel method was developed for the analysis of four β-blockers, namely sotalol, carteolol,
bisoprolol, and propranolol, in human urine by coupling carrier-mediated liquid phase …