Development and optimization of an ultra-fast microextraction followed by HPLC-UV of tetracycline residues in milk products

S Zergiebel, N Ueberschaar, A Seeling - Food Chemistry, 2023 - Elsevier
The present study developed a new ultra-fast microextraction (within 8 min) with acetonitrile
followed by gradient reversed-phase HPLC–UV method to determinate six tetracyclines …

Determination of six tetracyclines in eggs and chicken by dispersive liquid-liquid microextraction combined with high-performance liquid chromatography

Y Yang, S Yin, L Wu, Y Li, C Sun - Journal of AOAC International, 2021 - academic.oup.com
Background The wide usage of tetracyclines in livestock farming may result in drug residues
in foods. Therefore, it is necessary to develop reliable methods for the determination of …

Simplified extraction of tetracycline antibiotics from milk using a centrifugal ultrafiltration device

K Kishida - Food chemistry, 2011 - Elsevier
A simplified method was developed for the simultaneous determination of oxytetracycline,
tetracycline, chlortetracycline, and doxycycline in milk. Isolation of the target compounds was …

Mixed-mode fabric phase sorptive extraction of multiple tetracycline residues from milk samples prior to high performance liquid chromatography-ultraviolet analysis

E Agadellis, A Tartaglia, M Locatelli, A Kabir… - Microchemical …, 2020 - Elsevier
Herein, a new extraction mode of classical fabric phase sorptive extraction (FPSE), namely
mixed-mode strong cation exchanging FPSE is presented and evaluated for the first time for …

An overview of the main foodstuff sample preparation technologies for tetracycline residue determination

M Pérez-Rodríguez, RG Pellerano, L Pezza, HR Pezza - Talanta, 2018 - Elsevier
Tetracyclines are widely used for both the treatment and prevention of diseases in animals
as well as for the promotion of rapid animal growth and weight gain. This practice may result …

Determination of three tetracyclines in bovine milk using magnetic solid phase extraction in tandem with dispersive liquid-liquid microextraction coupled with HPLC

N Al-Afy, H Sereshti, A Hijazi, HR Nodeh - Journal Of Chromatography B, 2018 - Elsevier
A novel analytical method namely magnetic solid phase extraction in tandem with dispersive
liquid-liquid microextraction was developed and used for the extraction/preconcentration of …

A synergistic effect of hydrophobic deep eutectic solvents based on terpenoids and carboxylic acids for tetracycline microextraction

K Cherkashina, A Pochivalov, V Simonova… - Analyst, 2021 - pubs.rsc.org
Hydrophobic deep eutectic solvents were investigated for tetracycline microextraction. It was
found that a deep eutectic solvent consisting of thymol and octanoic acid provided a …

Isolation of tetracyclines in milk using a solid-phase extracting column and water eluent

N Furusawa - Talanta, 2003 - Elsevier
An isolating method using a solid-phase extraction (SPE) ISOLUTE® C8 endcapped syringe-
column for routine monitoring of residual tetracyclines (TCs)(oxytetracycline (OTC) …

Development and application of a dispersive liquid–liquid microextraction method for the determination of tetracyclines in beef by liquid chromatography mass …

SOS Mookantsa, S Dube, MM Nindi - Talanta, 2016 - Elsevier
A rapid, cost effective and environmentally friendly extraction method, based on dispersive
liquid–liquid microextraction (DLLME) was developed for the determination of six …

Development of an HPLC–UV method for the simultaneous determination of tetracyclines in muscle and liver of porcine, chicken and bovine with accelerated solvent …

H Yu, Y Tao, D Chen, Y Wang, Z Yuan - Food chemistry, 2011 - Elsevier
A simple and especially rapid method-using accelerated solvent extraction (ASE) and HPLC
has been developed for the quantitative determination of oxytetracycline, tetracycline …