Electron diffraction of 3D molecular crystals

A Saha, SS Nia, JA Rodríguez - Chemical Reviews, 2022 - ACS Publications
Electron crystallography has a storied history which rivals that of its more established X-ray-
enabled counterpart. Recent advances in data collection and analysis have sparked a …

Footprints of scanning probe microscopy on halide perovskites

S Gupta, S Bhattacharyya - Chemical Communications, 2024 - pubs.rsc.org
Scanning probe microscopy (SPM) and advanced atomic force microscopy (AFM++) have
become pivotal for nanoscale elucidation of the structural, optoelectronic and photovoltaic …

Emerging disordered layered-herringbone phase in organic semiconductors unveiled by electron crystallography

S Inoue, K Nikaido, T Higashino, S Arai… - Chemistry of …, 2021 - ACS Publications
The control of two-dimensional layered crystalline and/or liquid crystalline phases for π-
extended organic molecules is crucial for expanding the potential of organic electronic …

MicroED in natural product and small molecule research

E Danelius, S Halaby, WA van der Donk… - Natural product …, 2021 - pubs.rsc.org
Covering: 2013 to 2020 The electron cryo-microscopy (cryo-EM) method Microcrystal
Electron Diffraction (MicroED) allows the collection of high-resolution structural data from …

Photomechanochemical control over stereoselectivity in the [2+ 2] photodimerization of acenaphthylene

S Biswas, S Banerjee, MA Shlain, AA Bardin… - Faraday …, 2023 - pubs.rsc.org
Tuning solubility and mechanical activation alters the stereoselectivity of the [2+ 2]
photochemical cycloaddition of acenaphthylene. Photomechanochemical conditions …

Efficient free triplet generation follows singlet fission in diketopyrrolopyrrole polymorphs with goldilocks coupling

AM Levine, G He, G Bu, P Ramos, F Wu… - The Journal of …, 2021 - ACS Publications
Microcrystal electron diffraction, grazing incidence wide-angle scattering, and UV–vis
spectroscopy were used to determine the unit-cell structure and the relative composition of …

From Powders to Single Crystals: A Crystallographer's Toolbox for Small-Molecule Structure Determination

JA Newman, L Iuzzolino, M Tan, P Orth… - Molecular …, 2022 - ACS Publications
Although the crystal structures of small-molecule compounds are often determined from
single-crystal X-ray diffraction (scXRD), recent advances in three-dimensional electron …

Recent developments toward integrated metabolomics technologies (UHPLC-MS-SPE-NMR and MicroED) for higher-throughput confident metabolite identifications

R Ghosh, G Bu, BL Nannenga… - Frontiers in Molecular …, 2021 - frontiersin.org
Metabolomics has emerged as a powerful discipline to study complex biological systems
from a small molecule perspective. The success of metabolomics hinges upon reliable …

Microcrystal electron diffraction for molecular design of functional non-fullerene acceptor structures

S Halaby, MW Martynowycz, Z Zhu, S Tretiak… - Chemistry of …, 2021 - ACS Publications
Understanding the relationship between molecular structure and solid-state arrangement
informs about the design of new organic semiconductor (OSC) materials with improved …

Elucidation of diverse solid‐state packing in a family of electron‐deficient expanded helicenes via microcrystal electron diffraction (MicroED)

AE Samkian, GR Kiel, CG Jones… - Angewandte Chemie …, 2021 - Wiley Online Library
Solid‐state packing plays a defining role in the properties of a molecular organic material,
but it is difficult to elucidate in the absence of single crystals that are suitable for X‐ray …