Solid-state NMR spectroscopy is one of the most commonly used techniques to study the
atomic-resolution structure and dynamics of various chemical, biological, material, and …

In the last two decades, solid-state nuclear magnetic resonance (ssNMR) spectroscopy has
transformed from a spectroscopic technique investigating small molecules and industrial …

Internuclear distances represent one of the main structural constraints in molecular structure
determination using solid-state NMR spectroscopy, complementing chemical shifts and …

With the development of NMR methodology and technology during the past decades, solid-
state NMR (ssNMR) has become a particularly important tool for investigating structure and …

Proton detection developed in the last 20 years as the method of choice to study
biomolecules in the solid state. In perdeuterated proteins, proton dipolar interactions are …

With the recent advances in NMR hardware and probe design technology, magic-angle
spinning (MAS) rates over 100​ kHz are accessible now, even on commercial solid NMR …

The development of NMR crystallography methods requires a reliable database of chemical
shifts measured for systems with known crystal structure. We measured and assigned …

Selective recoupling of protons (SERP) is a method to selectively and quantitatively
measure magnetic dipole–dipole interaction between protons and, in turn, the proton–proton …

Solid-state nuclear magnetic resonance (NMR) often suffers from significant limitations due
to the inherent low signal sensitivity when low-γ nuclei are involved. Herein, we report an …

This primer article introduces a practical guide for setting up 1 H detection solid-state NMR
experiments under fast MAS conditions for small molecules. Sample independent …